Download or read online books in PDF, EPUB and Mobi Format. Click Download or Read Online button to get book now. This site is like a library, Use search box in the widget to get ebook that you want.

Purification of Laboratory Chemicals

Purification of Laboratory Chemicals Author W.L.F. Armarego
ISBN-10 9780128054567
Release 2017-03-14
Pages 1198
Download Link Click Here

Purification of Laboratory Chemicals, Eighth Edition, tabulates methods taken from literature for purifying thousands of individual commercially available chemicals. To help in applying this information, the more common processes currently used for purification in chemical laboratories and new methods are discussed. For dealing with substances not separately listed, a chapter is included setting out the usual methods for purifying specific classes of compounds. Features empirical formulae inserted for every entry References all important applications of each substance Updates and confirms the accuracy of all CAS registry numbers, molecular weights, original reference, and physical data Provides increased coverage of the latest commercial chemical products, including pharmaceutical chemicals, updated safety and hazard material, and expanded coverage of laboratory and work practices and purification methods



Purification of Laboratory Chemicals

Purification of Laboratory Chemicals Author W. L. F. Armarego
ISBN-10 9780123821614
Release 2013-01-01
Pages 1002
Download Link Click Here

A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readers on critical safety and hazards for the safe handling of chemicals and processes. The Seventh Edition is fully updated and provides expanded coverage of the latest commercially available chemical products and processing techniques, safety and hazards: over 200 pages of coverage of new commercially available chemicals since the previous edition. It will be accompanied by a CD-ROM database of all the substances in the book, fully searchable by chemical name, chemical group, CAS registry number, Beilstein number, etc. * The only comprehensive chemical purification reference, a market leader since 1966, Amarego delivers essential information for research and industrial chemists, pharmacists and engineers: '... (it) will be the most commonly used reference book in any chemical or biochemical laboratory' (MDPI Journal) * An essential lab practice and proceedures manual. Improves efficiency, results and safety by providing critical information for day-to-day lab and processing work. Improved, clear organization and new indexing delivers accurate, reliable information on processes and techniques of purification along with detailed physical properties. * The Sixth Edition has been reorganised and is fully indexed by CAS Registry Numbers; compounds are now grouped to make navigation easier; literature references for all substances and techniques have been added; ambiguous alternate names and cross references removed; new chemical products and processing techniques are covered; hazards and safety remain central to the book.



Purification of Laboratory Chemicals

Purification of Laboratory Chemicals Author W.L.F. Armarego
ISBN-10 9780123821621
Release 2012-10-17
Pages 1024
Download Link Click Here

A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readers on critical safety and hazards for the safe handling of chemicals and processes. The Seventh Edition is fully updated and provides expanded coverage of the latest commercially available chemical products and processing techniques, safety and hazards: over 200 pages of coverage of new commercially available chemicals since the previous edition. The only comprehensive chemical purification reference, a market leader since 1966, Amarego delivers essential information for research and industrial chemists, pharmacists and engineers: '... (it) will be the most commonly used reference book in any chemical or biochemical laboratory' (MDPI Journal) An essential lab practice and proceedures manual. Improves efficiency, results and safety by providing critical information for day-to-day lab and processing work. Improved, clear organization and new indexing delivers accurate, reliable information on processes and techniques of purification along with detailed physical properties The Sixth Edition has been reorganised and is fully indexed by CAS Registry Numbers; compounds are now grouped to make navigation easier; literature references for all substances and techniques have been added; ambiguous alternate names and cross references removed; new chemical products and processing techniques are covered; hazards and safety remain central to the book



Advanced Practical Organic Chemistry Third Edition

Advanced Practical Organic Chemistry  Third Edition Author John Leonard
ISBN-10 9781439860977
Release 2013-01-08
Pages 356
Download Link Click Here

Any research that uses new organic chemicals, or ones that are not commercially available, will at some time require the synthesis of such compounds. Therefore, organic synthesis is important in many areas of both applied and academic research, from chemistry to biology, biochemistry, and materials science. The third edition of a bestseller, Advanced Practical Organic Chemistry is a guide that explains the basic techniques of organic chemistry, presenting the necessary information for readers to carry out widely used modern organic synthesis reactions. This book is written for advanced undergraduate and graduate students as well as industrial organic chemists, particularly those involved in pharmaceutical, agrochemical, and other areas of fine chemical research. It provides the novice or nonspecialist with the often difficult-to-find information on reagent properties needed to perform general techniques. With over 80 years combined experience training and developing organic research chemists in industry and academia, the authors offer sufficient guidance for researchers to perform reactions under conditions that give the highest chance of success, including the appropriate precautions to take and proper experimental protocols. The text also covers the following topics: Record keeping and equipment Solvent purification and reagent preparation Using gases and working with vacuum pumps Purification, including crystallization and distillation Small-scale and large-scale reactions Characterization, including NMR spectra, melting point and boiling point, and microanalysis Efficient ways to find information in the chemical literature With fully updated text and all newly drawn figures, the third edition provides a powerful tool for building the knowledge on the most up-to-date techniques commonly used in organic synthesis.



Fine Chemicals Manufacture

Fine Chemicals Manufacture Author Andrzej Cybulski
ISBN-10 044482202X
Release 2001
Pages 551
Download Link Click Here

The sector of fine chemicals, including pharmaceuticals, agrochemicals, dyes and pigments, fragrances and flavours, intermediates, and performance chemicals is growing fast. For obvious reasons chemistry is a key to the success in developing new processes for fine chemicals. However, as a rule, chemists formulate results of their work as recipes, which usually lack important information for process development. Fine Chemicals Manufacture, Technology and Engineering is intended to show what is needed to make the recipe more useful for process development purposes and to transform the recipe into an industrial process that will be safe, environmentally friendly, and profitable. The goal of this book is to form a bridge between chemists and specialists of all other branches involved in the scale-up of new processes or modification of existing processes with both a minimum effort and risk and maximum profit when commercializing the process. New techniques for scale-up and optimization of existing processes and improvements in the utilization of process equipment that have been developed in recent years are presented in the book.



Practical Process Research and Development

Practical Process Research and Development Author Neal G. Anderson
ISBN-10 9780080514482
Release 2000-06-05
Pages 354
Download Link Click Here

This book provides a comprehensive, step-by-step approach to organic process research and development in the pharmaceutical, fine chemical, and agricultural chemical industries. Process R&D describes the steps taken, following synthesis and evaluation, to bring key compounds to market in a cost-effective manner. More people are being hired for work in this area as increasing numbers of drug candidates are identified through combinatorial chemistry and high-throughput screening. The book is directed to industrial (primarily organic) chemists, and academicians (particularly those involved in a growing number of start-up companies) and students who need insight into industrial process R&D. Current books do not describe hands-on, step-by-step, approaches to solving process development problems, including route, reagent, and solvent selection; optimising catalytic reactions; chiral syntheses; and "green chemistry." "Practical Process Research and Development" will be a valuable resource for researchers, managers, and graduate students. Provides insights into generating rugged, practical, cost-effective processes for the chemical preparation of "small molecules" Breaks down process optimization into route, reagent and solvent selection, development of reaction conditions, workup, crystallizations and more Includes over 100 tips for rapid process development Presents guidelines for implementing and troubleshooting processes



Experimental Organic Chemistry

Experimental Organic Chemistry Author Philippa B. Cranwell
ISBN-10 9781119952381
Release 2017-08-14
Pages 688
Download Link Click Here

Previous edition by Laurence M. Harwood, Christopher J. Moody, and Jonathan M. Percy.



Chemical Separations

Chemical Separations Author Clifton E. Meloan
ISBN-10 0471351970
Release 1999-10-06
Pages 768
Download Link Click Here

Performing effective chemical separations-a step-by-step guide to the most commonly used techniques. How do experienced analysts go about making a chemical separation work? Through precise, detailed coverage of the principles, equipment, and techniques involved, this combination laboratory manual and reference source gives readers a working knowledge of an impressive array of separation methods. In forty-two chapters, it explores all major categories of separation, including those involving phase changes, extraction, chromatography, ion-exchange resins, electric fields, flotation, membranes, and miscellaneous techniques. With an emphasis on everyday practice rather than theory, Chemical Separations explains the principles and parameters of these methods with a minimum of mathematics, while providing 59 specific experiments to demonstrate proper procedures. Drawn from well-known commercial and academic laboratories and approved by national standard-setting organizations, these experiments feature step-by-step protocols for each separation scheme, precise instructions on setting up the apparatus, and helpful checklists for essential chemicals and supplies. With Chemical Separations as their guide, laboratory analysts and newcomers to chemical analysis will learn how to obtain quality analysis using commercial products, natural samples, and proven real-world laboratory techniques.



Organicum

Organicum Author Heinz Becker
ISBN-10 9781483146287
Release 2013-10-22
Pages 768
Download Link Click Here

Organicum: Practical Handbook of Organic Chemistry focuses on the theory, laboratory practice, and aspects of technical use related to organic chemistry. This book discusses the standard apparatus for organic reactions, heating of inflammable liquids, performance of a simple distillation, and partition chromatography in separating columns. The time factor in organic chemical reactions, distribution of the electron density in organic molecules, and synthesis of ethers from alkoxides or phenoxides are also elaborated. This text likewise covers the mechanism of electrophilic aromatic substitution, quinones from aromatic hydrocarbons, and reduction of carbonyl compounds by means of complex hydrides. Other topics include the reaction with ammoniacal solution of a silver salt, preparation of the dimedone derivatives, and saturated aliphatic hydrocarbons. This publication is suitable for chemists and researchers conducting work in organic chemistry.



Prudent Practices in the Laboratory

Prudent Practices in the Laboratory Author The Committee on Prudent Practices in the Laboratory: An Update
ISBN-10 9780309138642
Release 2011-03-25
Pages 360
Download Link Click Here

Prudent Practices in the Laboratory--the book that has served for decades as the standard for chemical laboratory safety practice--now features updates and new topics. This revised edition has an expanded chapter on chemical management and delves into new areas, such as nanotechnology, laboratory security, and emergency planning. Developed by experts from academia and industry, with specialties in such areas as chemical sciences, pollution prevention, and laboratory safety, Prudent Practices in the Laboratory provides guidance on planning procedures for the handling, storage, and disposal of chemicals. The book offers prudent practices designed to promote safety and includes practical information on assessing hazards, managing chemicals, disposing of wastes, and more. Prudent Practices in the Laboratory will continue to serve as the leading source of chemical safety guidelines for people working with laboratory chemicals: research chemists, technicians, safety officers, educators, and students.



Advanced Practical Inorganic and Metalorganic Chemistry

Advanced Practical Inorganic and Metalorganic Chemistry Author R. John Errington
ISBN-10 0751402257
Release 1997-07-03
Pages 302
Download Link Click Here

While the boundaries between the areas of chemistry traditionally labeled as inorganic, organic and physical are gradually diffusing, the practical techniques adopted by workers in each of these areas are often radically different. The breadth and variety of research classed as "inorganic chemistry" is readily apparent from an inspection of some of the leading international journals, and can be quite daunting for newcomers to this domain who are likely to have only limited experience of the methodologies involved. This book has therefore been written to provide guidance for those unfamiliar with the techniques most often encountered in synthetic inorganic / metalorganic chemistry, with an emphasis on procedures for handling air-sensitive compounds. One chapter is devoted to more specialized techniques such as metal vapor synthesis, and a review of preparative methods for a selection of starting materials is included as an aid to those planning research projects. While this book is aimed primarily at postgraduate and advanced undergraduate students involved in inorganic research projects, synthetic organic chemists and industrial chemists will also find much useful information within its pages. Similarly, it serves as a useful reference source for materials and polymer scientists who wish to take advantage of recent progress in precursor synthesis and catalyst development.



Handbook of Water Purity and Quality

Handbook of Water Purity and Quality Author Satinder Ahuja
ISBN-10 0080921124
Release 2009-07-17
Pages 412
Download Link Click Here

This work provides those involved in water purification research and administration with a comprehensive resource of methods for analyzing water to assure its safety from contaminants, both natural and human caused. The book first provides an overview of major water-related issues in developing and developed countries, followed by a review of issues of sampling for water analysis, regulatory considerations and forensics in water quality and purity investigations. The subsequent chapters cover microbial as well chemical contaminations from inorganic compounds, radionuclides, volatile and semi-volatile compounds, disinfectants, herbicides, and pharmaceuticals, including endocrine disruptors, as well as potential terrorist-related contamination. The last chapter describes the Grainger prize-winning filter that can remove arsenic from water sources and sufficiently protect the health of a large number of people. - Covers the scope of water contamination problems on a worldwide scale - Provides a rich source of methods for analyzing water to assure its safety from natural and deliberate contaminants - Describes the filter that won the $1 million Grainger prize and thereby highlighting an important approach to remediation



Membrane Technology and Engineering for Water Purification

Membrane Technology and Engineering for Water Purification Author Rajindar Singh
ISBN-10 9780444634092
Release 2014-09-25
Pages 452
Download Link Click Here

Membrane Technology and Engineering for Water Purification, 2nd edition is written in a practical style with emphasis on: process description; key unit operations; systems design and costs; plant equipment description; equipment installation; safety and maintenance; process control; plant start-up; and operation and troubleshooting. It is supplemented by case studies and engineering rules-of-thumb. The author is a chemical engineer with extensive experience in the field, and his technical knowledge and practical know-how in the water purification industry are summarized succinctly in this new edition. This book will inform you which membranes to use in water purification and why, where and when to use them. It will help you to troubleshoot and improve performance and provides case studies to assist understanding through real-life examples. Membrane Technology section updated to include forward osmosis, electrodialysis, and diffusion dialysis Hybrid Membrane Systems expanded to cover zero liquid discharge, salt recovery and removal of trace contaminants Includes a new section on plant design, energy, and economics



Safe Storage of Laboratory Chemicals

Safe Storage of Laboratory Chemicals Author David A. Pipitone
ISBN-10 UOM:39015019425316
Release 1991-03-19
Pages 320
Download Link Click Here

Safe Storage of Laboratory Chemicals, Second Edition is a comprehensive guide which allows readers to assess and improve the safety of their laboratory operations when storing chemicals. By applying the information in this book, readers can create a safer place to work through a safer storage environment, wiser storage practices and procedures, informed personnel, and the intelligent use of information. There has seen a surge in the demand for chemical safety and information relating to a safe workplace. This book covers chemical storage, the requirements of OSHA and EPA, requirements in codes and standards for storage, and advances and applications for chemical health and safety. This book offers a balanced approach to the safe storage of laboratory chemicals. Applied knowledge for identifying chemical storage hazards, solutions and alternative measures for storing specific hazard classes of chemicals, and innovative case histories provide a wealth of information from which readers may draw to enhance the safety of their storage situations.



Sittig s Handbook of Toxic and Hazardous Chemicals and Carcinogens

Sittig s Handbook of Toxic and Hazardous Chemicals and Carcinogens Author Richard P. Pohanish
ISBN-10 9780323389693
Release 2017-06-05
Pages 3564
Download Link Click Here

Sittig's Handbook of Toxic and Hazardous Chemicals and Carcinogens, Seventh Edition, has proven to be a reliable, accessible, must-have reference on hazardous materials for over thirty years. This updated and revised seventh edition is the most comprehensive listing of the hazardous chemicals commonly used, transported, and regulated in industry and the workplace. Information is the most vital resource anyone can have when dealing with potential hazardous substance accidents, spillages, fires, or acts of terror. It is also essential for the safe day-to-day operation of chemical processes and environmental protection. Sittig's Handbook provides extensive data for over 2,200 chemicals in a uniform format, enabling fast and accurate decisions in any situation. The chemicals are presented alphabetically and classified as a carcinogen, hazardous substance, hazardous waste, or toxic pollutant. This new edition contains expanded and reviewed information for each chemical listed (including chemicals classified as WMD) and has been updated to keep pace with world events, standards, and regulations. This seventh edition includes over 100 new records, and every single record has been checked and updated as necessary. Enables readers to quickly and reliably find the chemical they are looking for, with a full range of synonyms for each chemical, including trade names and CAS index Features relevant data for the US and EU included throughout, along with the essential chemical hazard information applicable worldwide Provides a trusted source of information for first-line responders (emergency services), industry, logistics companies, scientists, and environmental protection organizations Contains expanded information for each chemical listed (including chemicals classified as WMD) and has been updated to keep pace with world events, standards, and regulations



Hazardous Laboratory Chemicals Disposal Guide Third Edition

Hazardous Laboratory Chemicals Disposal Guide  Third Edition Author Margaret-Ann Armour
ISBN-10 1420032380
Release 2016-04-19
Pages 592
Download Link Click Here

A perennial bestseller, Hazardous Laboratory Chemicals Disposal Guide, Third Edition includes individual entries for over 300 compounds. The extensive list of references has been updated and includes entries for 15 pesticides commonly used in greenhouses. Emphasis is placed on disposal methods that turn hazardous waste material into non-toxic products. These methods fall into several categories, including acid/base neutralization, oxidation or reduction, and precipitation of toxic ions as insoluble solids. The text also provides data on hazardous reactions of chemicals, assisting laboratory managers in developing a plan of action for emergencies such as the spill of any of the chemicals listed.



Trends in Organometallic Chemistry Research

Trends in Organometallic Chemistry Research Author Marin A. Cato
ISBN-10 1594544948
Release 2005
Pages 214
Download Link Click Here

Organometallic chemistry is based on the reactions and use of a class of compounds (R-M) that contain a covalent bond between carbon and metal. They are prepared either by direct reaction of the metal with an organic compound or by replacement of a metal from another organometallic substance. Research in organometallic chemistry is also conducted in the areas of cluster synthesis, main-group derivatives in unusual oxidation states, organometallic polymers, unstable organometallic compounds and intermediates in matrices, structure determination of organometallic compounds in the solid state [X-ray diffraction] and gaseous states [electron diffraction], and mechanisms of reactions of transient silylenes and related species. . In addition to the traditional metals and semimetals, elements such as selenium, lithium and magnesium are considered to form organometallic compounds, e.g. organomagnesium compounds MeMgI, iodo(methyl)magnesium and diethylmagnesium which are Grignard reagents an organo-lithium compound BuLi butyllithium; Organometallic compounds often find practical use as catalysts, the processing of petroleum products and the production of organic polymers.